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Scanning Electron Microscopy (SEM) Instrumentation and Application

Posted by Unknown at 11:22 PM

Vital parts of all SEMs involve the next:
  1. Electron Resource (\"Gun\")
  2. Electron Lenses
  3. Sample Stage
  4. Sensors for all indicators of interest
  5. Display / Data output units
  6. Infrastructure Demands:

    • Energy Supply
    • Vacuum Method
    • Cooling method
    • Vibration-cost-free ground
    • Room free of charge of ambient magnetic and electrical fields

SEMs generally have at minimum a person detector (normally a secondary electron detector), and most have more sensors. The unique abilities of a certain instrument are critically dependent on which detectors it accommodates. 


Applications
The SEM is routinely used to create large-resolution photos of styles of objects (SEI) and to show spatial versions in chemical compositions: one) obtaining elemental maps or spot chemical analyses using EDS, two)discrimination of phases primarily based on necessarily mean atomic quantity (normally related to relative density) using BSE, and 3) compositional maps dependent on distinctions in trace aspect \"activitors\" (generally transition steel and Rare Earth factors) utilizing CL. The SEM is also broadly applied to establish phases primarily based on qualitative chemical evaluation and/or crystalline construction. Specific measurement of really compact features and objects down to 50 nm in dimension is also accomplished using the SEM. Backescattered electron pictures (BSE) can be employed for fast discrimination of phases in multiphase samples. SEMs outfitted with diffracted backscattered electron detectors (EBSD) can be employed to take a look at microfabric and crystallographic orientation in several resources.